SCIENCE AND TECHNOLOGY OF CEREALS, OILS AND FOODS

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  • 1  Simultaneous determination of deoxynivalenol and ramification in wheat by immune affinity column and high performance liquid chromatography
    王培 徐广超 尹丽梅 黎睿 谢刚
    2015, 23(1):63-66.
    [Abstract](2314) [HTML](0) [PDF 1.59 M](2681)
    Abstract:
    The method to determine deoxynivalenol (DON), 3-acetyl- deoxynivalenol (3-A-DON) and 15-acetyl-deoxynivalenol (15-A-DON) in wheat simultaneously by immune affinity column clean-up and high performance liquid chromatography was established. The wheat samples were extracted by ultrapure water, cleared up with the immuno-affinity column (IAC). After drying and constant volume, three toxins, DON、3-A-DON and15-A-DON, were detected simultaneously by high performance liquid chromatograph with UV detector, and compared with that by Liquid chromatography mass spectrometry. The result showed that the detection limit of method was 100 μg/kg for DON, 3-A-DON and 15-A-DON respectively. Recovery rates in wheat spiked with DON, 3-A-DON, and 15-A-DON, ranged from 86.6% to 96.5%. The variation coefficient was less than 10%. This method was suitable for determination of DON, 3-A-DON, and 15-A-DON in wheat, with the advantages of simplicity, rapidness, sensitivity and good selectivity, veracity and precision.
    2  Effects of milling methods on the processing quality of glutinous rice flour
    ZHOU Xian-qing XIA Wen-wen ZHANG Yu-rong HU Yu-ming
    2014, 22(1):7-13.
    [Abstract](2026) [HTML](0) [PDF 0.00 Byte](1803)
    Abstract:
    The effect of milling methods on the quality of glutinous rice flour was studied by analyzing the physicochemical characteristics, the thermodynamic properties and the texture of glutinous rice flour milled by different methods. The results showed that the difference between the effects of different milling methods on the quality of glutinous rice flour was significant. The moisture content of the flour was easy to control with better color, lower ash content, acidity, fatty acid value, solubility and retrogradation, and better swelling degree when the wet milling method was used. However, no significant differences were observed in their transparency, water retention and the thermodynamic properties. The quality of glutinous rice flour was the best one produced by wet milling method in texture.
    3  Research progress on the applications of simulation technology in grain storage ecosystem
    Wu Zi-dan Zhao Hui-yi Cao yang Li Fu-jun Wei Lei
    2014, 22(1):1-6.
    [Abstract](2015) [HTML](0) [PDF 0.00 Byte](1846)
    Abstract:
    The simulation technology has been applied in grain storage ecosystem following the development of information technology, and has been an important tool for the research on interactive influence among multi-factors. Combining with the structure and characters of grain storage ecosystem, the research progress and application status of the followed area was introduced in detail: environment and ecology subsystem, computer simulations for grain pile non-biological field under no manual intervention conditions, simulation research in mechanical ventilation of grain storage, computer simulation research for the detection and precontrol of storage pests, and simulation research for growth model and precontrol of storage microorganisms.The characteristics of individual field effect on grain storage ecosystem will be more unequivocal by using simulation technology. Multi-parameter optimized control strategy for grain storage ecosystem will be formed gradually based on the research of multi-fields coupling theory.
    4  Discussion on problems in development of rice processing industry in China
    谭斌 吴娜娜 谭云
    2014, 22(2):1-5.
    [Abstract](2010) [HTML](0) [PDF 0.00 Byte](1785)
    Abstract:
    Rice is a traditional staple food in China,and it's very important for the production of grain.At present,China is in a critical period of industrial structure and consumption structure transformation.Rice processing industry has entered into a new development stage of the pursuit of delicious,safe and secure,nutrition and health,convenience and diversification.The strategic position of rice in the staple food industry in China and in the world,and the development status of rice processing industry in China were studied.The problems in the development of rice processing industry nowadays were also discussed.
    5  A rapid method for the determination of edible oil iodine value
    杨丽 纪东彬 薛敦辉 陈蓉 杜虹颖 卢玮彤 关杏彬 高静雯
    2014, 22(2):61-63.
    [Abstract](2004) [HTML](0) [PDF 0.00 Byte](1681)
    Abstract:
    The improved determination method was tested by adding Wijs reagent and 10 mL 3% magnesium acetate solution as catalyst reacting for 13 min,according to the principle and operation method of national standard for determination of iodine value in edible oil(Wijs method).The results showed that there was no great difference between the two methods with the relative error less than 2%.It indicated that catalyst magnesium acetate had no adverse effect on the accuracy of determination results.The improved method,possessing less toxicity,good accuracy and reliability,is a rapid method for determination of iodine value in edible oil.
    6  Determination of tannin in fresh bamboo shoots by Folin-Ciocalteu colorimetric spectrophotometry
    FEI Jian-feng XIE Jia-ni LIU Juan-juan FANG Xu-bo CHEN Ke-ke CHEN Na
    2013, 21(4).
    [Abstract](1690) [HTML](0) [PDF 0.00 Byte](0)
    Abstract:
    实验采用Folin-Ciocalteu比色分光光度法测定新鲜竹笋中单宁的含量.结果显示:新鲜竹笋待测液加入Folin-Ciocalteu显色剂2 mL,9%的Na2CO3溶液5 mL,定容混匀后于40℃静置60 min,并在770 nm处测定其光密度值(OD值),经计算得到新鲜毛竹冬笋和毛竹春笋单宁质量分数分别为0.131 4%、0.330 5%.以单宁为标样,单宁量在0.000~0.020 mg/mL范围之内服从比耳定律,回归方程y=98.957x+0.029,相关系数R2 =0.992 7,据此线性回归方程定量测定鲜笋中的单宁,该方法具有方便、操作简单、精密度高、稳定性好及准确可靠等优点.
    7  Extraction of protein from corn germ by reverse micelle and its functionality
    任婷婷 吕双双 李书国
    2014, 22(2):80-84.
    [Abstract](1682) [HTML](0) [PDF 0.00 Byte](1584)
    Abstract:
    Extraction of protein from corn germ by AOT/isooctane reversed micellar extraction and its processing functionality were studied. The effects of dosage of cellulase, AOT mass concentration, KCl concentration, pH of buffer solution and W0 on the forward extraction rate of the protein, and the effects of extraction time, KCl concentration, pH of buffer solution on the backward extraction rate were investigated. The optimum forward extraction conditions were determined: dosage of cellulase 4 000 IU/g corn germ, AOT mass concentration 3 g/50 mL isooctane, pH 6, KCl concentration 0.1 mol/L, W0 25. The optimum backward extraction conditions were as follows: KCl concentration 0.5 mol/L, pH 10.5, and extraction time 40 min. Some processing functionality of corn germ protein was studied. The result showed that oil absorptivity (2.9 mL/g), emulsifiability (54.5%),emulsion stability (86.5%) and foam stability (58.3%) were good. But water absorptivity and foamability was slightly poorer than rice protein. Corn germ protein has higher nutritive value and perfect processing functionality; therefore it can be used in food industry.
    8  Optimization of fermentation conditions of lactic acid bacteria exopolysaccharide and the effect on the steamed bread quality
    杨晓露 李志建 邵源 刘长虹 卞科
    2014, 22(2):92-94.
    [Abstract](1606) [HTML](0) [PDF 0.00 Byte](1544)
    Abstract:
    A lactic acid bacteria with high yield of exopolysaccharide (EPS) named L1 was isolated from sourdough and identified as lactobacillus plantarum. The results showed that the highest exopolysaccharide yield was obtained when the carbon-nitrogen ratio in medium was 2∶1 at initial pH 6 incubated for 18 h at 30 ℃. The specific volume and sensory score of steamed bread with L1 EPS increased obviously and whiteness increased slightly.
    9  Talk about the characteristics of grain storage in squat silo
    张来林 蔡育池 许国川 苏瑜敏 刘育森
    2019, 27(5):97-100.
    [Abstract](1499) [HTML](0) [PDF 198.67 K](2840)
    Abstract:
    According to the structure of squat silo, the characteristics of large grain heap and experience in the past 20 years, the characteristics of grain storage in squat silo were summarized. By utilizing favorable conditions for playing good thermal insulation of squat silos and complete facilities, improving the management mode during processing,the grain temperature in squat silo was controlled, therefore some problems,such as agglomeration, moisture condensation, grain hanging on the silo wall, were avoided to ensure the safety of grain storage in squat silo.
    10  Technical analysis of Design code for vegetable oil depot
    杨书民
    2015, 23(1):102-104.
    [Abstract](1467) [HTML](0) [PDF 1.10 M](2225)
    Abstract:
    Some provisions, which was easy to cause confusion, in Design code for vegetable oil depot (LS 8010-2014) implemented on March 1, 2014 were analyzed in technical aspect. The provisions included determination of the flash point of vegetable oil, fire hazard classification, the total capacity of the tank group, tank spacing, tank type and ratio of height to diameter and vegetable oil tank can installed without a lightning rod etc. So the relevant personnel within the industry can correctly understand and use the code.
    11  Comparison of the Nutritional Values of Quinoa in Four Different Colors
    LIU Jian-lei ZHANG Dong WANG Wen-juan YANG Wei-qiao SUN Hui DUAN Xiao-liang
    2024, 32(6):134-142. DOI: 10.16210/j.cnki.1007-7561.2024.06.016
    [Abstract](1316) [HTML](472) [PDF 542.64 K](752)
    Abstract:
    To compare the nutritional values of different colored quinoa, four main varieties of white, black, red, and gray quinoa from China's major quinoa-producing provinces were selected. Their nutrient contents were comprehensively compared, and hierarchical cluster analysis was further used to classify the samples and nutritional indicators. The results showed that compared with staple foods such as wheat flour and rice, as well as other grains like oats, buckwheat, millet, and highland barley, quinoa had higher crude protein, crude fat, ash, insoluble dietary fiber (IDF), P, K, Zn, and lower total starch content. Quinoa had higher vitamin B1 and B2 levels than wheat flour and rice but lower levels than buckwheat, millet, and highland barley. Among the different colored quinoa, gray quinoa had the greatest distinction from the other three colors, while red and black quinoa were the most similar. The contents of total dietary fiber (TDF), IDF, Cu, Zn, total starch, Mn, and K were higher in dark-colored quinoa such as black and red varieties. The contents of vitamin B1, soluble dietary fiber (SDF), and Se were higher in light-colored quinoa such as gray and white varieties. The contents of total flavonoids, Fe, and crude fat were higher in gray and red quinoa. The contents of vitamin B2 and crude protein were higher in white and red quinoa. The contents of Ca, Mg, and P were higher in gray and black quinoa. In summary, the nutritional characteristics of different colored quinoa were complementary to some extent, and a mixture of different colored quinoa could provide more comprehensive nutritional profiles.
    12  Study on the expression of regulation of two strong promoters in bacillus subtilis
    周艳敬 常晓娇 吴子丹 伍松陵 孙长坡
    2015, 23(2):68-72.
    [Abstract](1315) [HTML](0) [PDF 2.62 M](2117)
    Abstract:
    The effect of two kinds of constitutive strong promoters P43 and PlapS on regulation of heterologous gene was compared on the expression level of ZEN degrading enzyme gene ZLHY6 and the enzyme activity evaluation. The degrading enzyme gene regulated by PlapS received efficient expression in bacillus subtilis 168, and the degrading enzyme activity reached the highest level of 219.02 U/mL after fermentation for 12 h. Moreover, the genetic stability of ZEN degrading enzyme gene expression vector pWBZ7 regulated by PlapS in Bs 168 lays a foundation for efficient expression and secretion of degrading enzyme.
    13  Effect of propylene glycol alginate on rheological and baking properties of dough
    刘海燕 逄锦龙 王小霞 刘然然 代增英 王晓梅
    2017, 25(6):1-4.
    [Abstract](1296) [HTML](1212) [PDF 963.70 K](1898)
    Abstract:
    The effect of propylene glycol alginate (PGA) with different percentages (0.1%、0.2%、0.3% and 0.4%) on rheological properties and baking properties of dough was analyzed by farinograph,extensograph and texture analyser.The results showed that:PGA could improve the farinograph properties and extensograph properties of dough,such as water absorption,stability time,flour evaluation index,dough extension,extension resistance and stretch ratio.PGA could increase the specific volume of bread,significantly improve the springiness,the taste and sensory score of bread,and reduce the hardness of bread.The bread with 0.2%~0.3% PGA had the optimal quality.
    14  Research Progress on the Toxicity and Detoxification of T-2 Toxin
    SONG Jia FAN Huan YAN Xue WANG Wen-jie ZHAO Chen
    2020, 28(5):194-199.
    [Abstract](1267) [HTML](0) [PDF 976.53 K](1415)
    Abstract:
    T-2 toxin is a secondary metabolite produced by Fusarium spp., and belongs to the type A mycotoxins in the cephalosporins family. T-2 toxin is highly toxic, and it pollutes not only crops in the field, but also granary which leads the post-harvest lost of grain, furthermore, it causes huge damage to human and animal health. Therefore, it becomes world widely the target to be prevented and controlled in the food industry and livestock industry in recent years. At present, the research on the biological toxicity of T-2 toxin is more indepth, but it still lacks adequate study on detoxification of T-2 toxin, especially the biological detoxification. The harm, mechanism and physical, chemical and biological methods of detoxification of T-2 toxins were reviewed. Focusing on the acquisition of efficient detoxification enzymes and the development of detoxification processes are conducive to the healthy development of multiple industries in China, such as grain industry, livestock industry, and by-product deep processing.
    15  Analysis of sterols content and composition in special vegetable oils
    朱琳 薛雅琳 张东 徐冉 柴杰
    2015, 23(2):49-52.
    [Abstract](1226) [HTML](0) [PDF 2.64 M](2079)
    Abstract:
    The total content of sterols in 4 kinds of special vegetable oils,i.e. peony seed oil, walnut oil, pumpkin seed oil and grape seed oil, and their composition were analyzed by gas chromatography. The result showed that sterols content in peony oil was 240.0 mg/100 g, of which the main components were β-sitosterol, Δ5, 23-stigmastadienol and Δ5-avenasterol; In walnut oil, the total content of sterols was 100.5 mg/100 g and β-sitosterol was the main component; In pumpkin seed oil,the total content of sterols was 299.6~358.4 mg/100 g, and the main components were β-sitosterol, Δ5,24-stigmastadienol and Δ7-avenasterol; In grape seed oil,the total content of sterols was 222.5~234.9 mg/100 g, and the main components were β-sitosterol, campesterol sterol and stigmasterol. The research provides basic data for development and process of special vegetable oil.
    16  Research on stored grain insects in Jiangxi province
    贺培欢 曹 阳 林丽莎 章 妺 李 娜 郑 丹 汪中明
    2017, 25(4):76-81.
    [Abstract](1208) [HTML](1134) [PDF 927.44 K](1712)
    Abstract:
    The insects in stored grain of grain depots, grain processing factories, feed mills and farmers household in 5cities in Jiangxi province were investigated.60 species of stored grain insects were collected, most of them were coleopteran reached to 42 species,accounting for 70%. Tribolium castaneum Herbst and Rhizopertha dominica Fabricius were most common stored grain insects in this area, both with the total occurrences of 69.6%. Total occurences of 12 species of main pests were generally over 10%. The results also showed there were only 5.4 species per depots on average in grain depots. Compared with grain depots, more insect species were found in grain-processing factories, feed mills and farmers household, about 11.8 species per survey spot on average. It was found that there were many species of natural enemy of stored grain pests in Jiangxi province, the main species were parasitic flies, stinkbugs, pseudoscorpions and predatory mites, which had natural advantages of biological control of stored grain pests. Moreover, Cryptolestes pusilloides (Steel et Howe) was collected in Jiangxi province for the first time.
    17  Analysis on flour and bread quality of new wheat No.26 yielded from different milling sections
    刘磊 齐学文 周裔彬 姚大年 郑文寅 胡承霖
    2014, 22(2):12-15.
    [Abstract](1160) [HTML](0) [PDF 0.00 Byte](1415)
    Abstract:
    The quality of wheat flour presents some differences due to the different extracting section of the milling process. Compared with the control bread flour, the new wheat No.26 as the raw material was milled by laboratory mill to extract flour from three break systems and three reduction systems. The milling flow for bread flour was designed by determining the main component, farinograph parameters, RVA pasting properties and bread TPA parameters of the flour. The results showed that the protein and wet gluten content in the flour from break system was higher than that from reduction system, that from head break system lower than that from tail break system, and that from head reduction system higher than that from tail reduction system. The dough development time,stabilization time, peak viscosity, setback of the flour from each system, and the elasticity and resilience of bread was consistent with the change of protein content. The ash content of the flour from 1M was the lowest, both water absorption and fat content of the flour from 3M was the highest, while the bread hardness, chewiness, degree of softening and breakdown of the flour from 3B were the lowest. Compared with the control group bought from market, the flour from tail break system and from head reduction system could be utilized as bread flour. The flour from 3B was the best among break system and that from 1M was the best among reduction system.
    18  Optimization of formula of composite stabilizer in jujube soy milk by response surface methodology
    曾 璟 胡洁芳 沈勇根 周 明 艾啸威
    2017, 25(6):13-20.
    [Abstract](1150) [HTML](1198) [PDF 3.28 M](1785)
    Abstract:
    The effect of complex emulsifiers-thickeners on the stability of compound protein beverage made of concentrated jujube juice and soybean was discussed.Based on the single factor experiment,the best ratio of the thickener and their quantity range were chosen.The effects of compound thickener,sucrose fatty acid ester,distilled glycerin monostearate and their interaction on the stability of the protein milk containing jujube and soybean were analyised by Box-Benhnken response method.The quadratic polynomial regression equation prediction model was obtained by Design Expert software (8.0.6.1).The results showed that the stability of the jujube-soybean milk was improved effectively by the compound stabilizer contained 0.06% compound thickeners (xanthan:guar gum:sodium carboxymethyl celubse=4:2:3),0.10% sucrose fatty acid ester and 0.04% distilled glycerin monostearate,and the product tastes exquisite with the best quality.
    19  Research on adsorption removal of phthalic acid esters in oil
    张明明 刘玉兰 杨金强 刘必衍
    2015, 23(5):32-36.
    [Abstract](1133) [HTML](0) [PDF 5.29 M](2733)
    Abstract:
    The effects of adsorbent type (10 types of adsorbents), adsorbent dosage, adsorption temperature and adsorption time on the removal of 5 plasticizers in camellia oil were investigated. The results showed that the optimal adsorbent was H-2 activated carbon, followed by 55F-A activated carbon, 55JN-C activated carbon, attapulgite and activated clay, when the adsorption temperature was 110 ℃, the adsorption time was 30 min and the dosage of adsorbent was 2.0%. Under the optimal condition (the adsorption temperature was 130 ℃, the adsorption time was 50 min and the dosage of the H-2 activated carbon was 2.0%), the removal rates of DMP, DEP, DIBP, DBP and DEHP were 76.7%, 50.7%, 52.4%, 22.2% and 6.1%, respectively. Removing DMP, DEP and DIBP from camellia oil by adsorption was efficient, while inefficient for high molecular weight DBP and DEHP.

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