SCIENCE AND TECHNOLOGY OF CEREALS, OILS AND FOODS

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Determination of D chiro inostiol in buckwheat by high performance capillary electrophoresis with indirect ultraviolet detection
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    Abstract:

    D chiro inostiol in buckwheat was determined by high performance capillary electrophoresis (HPCE) with ultraviolet detector, with100 mmol/L borate buffer, voltage 10kV and detection wavelength 195 nm. The results showed that the linear range was 0.1~150 mg/mL with correlation coefficients more than 0.999 and the detection limit less than 0.02 mg/mL (RS/N=3).The average recoveries were in the range of 9%~108%, with the relative standard deviation (RSD) 4.3%. This method is convenient, accurate and reliable, which can decrease the cost and pollution, increase the efficiency with aqueous solution as moving phase.

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  • Received:
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  • Online: January 25,2018
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