SCIENCE AND TECHNOLOGY OF CEREALS, OILS AND FOODS

1. Chinese Science Citation Database (CSCD)
2. A Guide to the Core Journals of China (2023)
3. The Key Magazine of China Science and Technology
4. Chinese Applied Core Journals (CACJ)
5. " 2022、2023 Bilingual Communication Project for Chinese STM Journals"
6. " 2022、2024 China Fine Periodical Exhibition"
7. Elsevier-Scopus Database
8. Directory of Open Access Journals (DOAJ)
9. EBSCO Research Database
10. Chemical Abstracts (CA)
11. Food Science and Technology Abstract (FSTA)
12. CAB International (CABI) Database
13. Japan Science and Technology Agency (Chinese Bibliographic Database) (JSTChina)
14. Ulrich’s Periodicals Directory (UPD)

Determination of 5 organophosphorus pesticides residues in paddy by dispersive solid phase extraction- gas chromatography
DOI:
Author:
Affiliation:

Clc Number:

Fund Project:

  • Article
  • |
  • Figures
  • |
  • Metrics
  • |
  • Reference
  • |
  • Related
  • |
  • Cited by
  • |
  • Materials
  • |
  • Comments
    Abstract:

    A fast method was developed for the determination of 5 organophosphorus pesticide residues (dimethoate, chlorpyrifos, malathion, isocarbophos, fenitrothion) in paddy by neutral alumina dispersive solid phase extraction - gas chromatography with flame photometric detector (DSPE-GC-FPD). The powdered samples were extracted with acetonitrile. The extract was purified by neutral alumina DSPE,dried by nitrogen evaporator with water bath at 70 ℃,and dissolved by acetone and determined by capillary gas chromatograph with flame photometric detector(CGC-FPD). The results showed that the 5 organophosphorus pesticide showed a good linear relationship in the range of 0.05~5.00 μg/mL, all of their linear correlation coefficients were 0.999 9, the limit of detection was 0.002 mg/kg, and the minimum quantitative limit was 0.007 mg/kg. The spiked recoveries at three levels of standard additions in paddy were between 97.7%~108.0%, and the RSDs (n=6) were between 0.8%~5.7%. This method could be used to determine 5 organophosphorus pesticide residues in paddy at the same time.

    Reference
    Related
    Cited by
Get Citation
分享
Article Metrics
  • Abstract:
  • PDF:
  • HTML:
  • Cited by:
History
  • Received:
  • Revised:
  • Adopted:
  • Online: September 02,2015
  • Published: